2.4c) consistent with deformation on the {110}〈1
Deformation of Bridgmanite.
A few deformation studies exist on Brg, using the DAC (Meade et al., 1995; Meade & Jeanloz, 1990; Merkel et al., 2003; Miyagi & Wenk, 2016; Wenk et al., 2004; Wenk, Lonardelli, et al., 2006), a modified large‐volume press assembly (Chen et al., 2002; Cordier et al., 2004; Tsujino et al., 2016), and the RDA (Girard et al., 2016). Early DAC deformation studies of Brg found no evidence for texture development in decompressed samples (Meade et al., 1995) or in in‐situ measurements of samples deformed outside the Brg stability field (Merkel et al., 2003). In contrast, Wenk et al. (2004) and Wenk, Lonardelli, et al. (2006) reported significant texture development in Brg and Brg + Fp aggregates synthesized in‐situ in the DAC from different starting materials. Different textures were observed, depending on starting material, and it was suggested that textures could be explained by slip on (010)[100], (100)[010], and (001)(110). Twinning on (110) was also suggested as a mechanism for texture development (Wenk et al., 2004). However, subsequent measurements by Miyagi & Wenk (2016) showed that the wide range of textures observed in Wenk et al. (2004) were likely due to the phase transformation from varied starting materials. Synthesis of bridgmanite from enstatite results in a strong (001) transformation texture while synthesis from olivine or ringwoodite results in a weak (100) transformation texture (e.g., Figure 2.4d; Miyagi & Wenk, 2016).
Twinning has been documented in Brg and is associated with the phase transformation to Brg but also has been observed in stress relaxation experiments. TEM studies of recovered samples from high‐pressure experiments documented reflection twins on (110) and (112) (Martinez et al., 1997; Y. Wang et al., 1990, 1992). In‐situ stress relaxation measurements at 20 GPa and 1073 K using the LVP and also found evidence for activity of (110) twinning (Chen et al., 2002).
Experimental evidence for slip systems in Brg generally shows either deformation on (001) planes or (100) planes. Several studies have documented texture, line broadening, or TEM observations consistent with slip on (001) planes. Cordier et al. (2004) suggested (001)[100] and (001)[010] dislocations based on x‐ray line broadening analysis of samples recovered from a large‐volume press deformation experiment at 25 GPa and 1700 K. A TEM study by Miyajima et al. (2009) documented 〈110〉 Burgers vectors, indicating that the likely slip plane is (001). Room‐temperature DAC experiments observed a (001) maximum at pressures < 55 GPa and room temperature (Figure 2.4e), consistent with dominant (001) slip, with some combination of slip in [100], [010], and 〈110〉 directions (Miyagi & Wenk, 2016). However, after laser annealing and compression above 55 GPa, Miyagi & Wenk (2016) observed a (100) texture maximum (Figure 2.4f) consistent with slip on (100). Interestingly, numerical modeling using first principles and the Peierls‐Nabarro model suggests that at pressures < 30GPa, slip on (001)〈110〉 is dominant, but at higher pressures (100)[010] slip is more active in Brg (Mainprice et al., 2008). Recent shear deformation experiments to 80% strain at 25 GPa and 1873 K in the D‐DIA with a Kawai type assembly showed textures consistent with slip on (100)[001] (Figure 2.2g; Tsujino et al., 2016).
Generally, numerical models to evaluated slip system strengths find that (010)[100] and (100)[010] should be the easiest slip systems (Ferré et al., 2007; Gouriet et al., 2014; Hirel et al., 2014). So far, experiments have not documented evidence for (010) slip. One should note, however, that due to geometric constraints and the number of symmetric variants, the easiest slip systems is not always most active during deformation (Mainprice et al., 2008). Based on experiments, it appears that at lower pressures and room temperature, slip on (001) dominates, but at higher pressure and at higher temperature (100), slip appears to be active (Table 2.1). However, systematic studies of slip system changes in Brg as a function of temperature, pressure, strain rate, and composition have not been performed and remain technically challenging. Furthermore, numerical simulations indicate that in the lower mantle, pure‐climb creep (Nabarro, 1967) may be the dominant deformation mechanism (Boioli et al., 2017; Cordier & Goryaeva, 2018; Reali et al., 2019), but due to experimental limitations, this deformation regime has yet to be explored in bridgmanite.
2.4.3 Post‐Perovskite
Although many studies have focused on slip systems and texture development in MgSiO3 pPv and pPv analogs, the dominant slip systems are still debated. In general, the slip plane tends to be better constrained than slip direction. Nonetheless, three sets of dominant slip systems have been proposed for pPv. These are slip on (010) planes, slip on (100), and/ or {110}〈1
Early studies proposed that slip should occur on the (010) plane based on the fact that this coincides with the layering of the SiO6 octahedra in the pPv structure (Iitaka et al., 2004; Murakami et al., 2004; Oganov & Ono, 2004). Several theoretical calculations have also supported slip on (010) in pPv or pPv analog materials (Carrez et al., 2007b, 2007a; Goryaeva et al., 2015a, 2015b, 2016, 2017; Metsue et al., 2009). Experimental evidence for slip on the (010) plane in pPv is limited to the CaIrO3 analog. Due to the fact that it is stable in the pPv structure at ambient or near‐ambient conditions (Rodi & Babel, 1965), CaIrO3 has been the most studied for deformation mechanisms of the pPv structured compounds. In compression studies, CaIrO3 develops a maximum at (010) in the IPF (Figure 2.5a; Hunt et al., 2016; Miyagi, Nishiyama, et al., 2008; Niwa et al., 2007). A wide range of experiments using the DAC, D‐DIA, and other large volume apparatus at pressure and temperature condition up to 6 GPa and 1300 K over a range of strain rates all find dominant slip on (010)[100] and (010)<u0w> (Table 2.1; Hunt et al., 2016; Miyagi, Nishiyama, et al., 2008; Miyajima et al., 2006; Miyajima & Walte, 2009; Niwa et al., 2007; Walte et al., 2007, 2009; Yamazaki et al., 2006).
Figure 2.5 Summary of the various textures types observed in post‐perovskite structured compounds over a range of pressure and temperature conditions. Textures are represented as equal area, upper hemisphere projection, inverse pole figures of the compression direction. Scale bar is in multiples of random distribution.
Evidence for (100) or and/ or {110}〈1