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Spectroscopy for Materials Characterization


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is the envelope of the many replicas. Neglecting the vibrations, the more common homogeneous lineshape is the Lorentzian, whereas the inhomogeneous lineshape is the Gaussian. The intermediate lineshape that is a Gaussian convolution of Lorentzian lineshapes is known as Voigt lineshape. The analytic forms of these functions are:

      (1.77)equation

      this lineshape is centered at ν 0 and is characterized by a full width at half maximum (FWHM) of the amplitude equal to 2A;

      this is centered at ν 0 and has FWHM images; finally, the Voigt function can be defined as

      (1.79)equation

      where the Gaussian and Lorentzian contributions have been introduced. The final shape of the Voigt function depends on the balance between the FWHM of the two composing contributions.

      To go deeper into the homogeneous lineshape features, the case of a molecular system has to be considered. It is then necessary to determine its electronic states in detail. First of all, the molecule is a many‐body system constituted by the electrons, the nuclei (it is useful to consider this unit for spectroscopic aims, associating the constituent parts: protons and neutrons, motion) and their motion and interaction. The more general Hamiltonian for this system is

      (1.80)equation

      where the subscripts label electrons’ (e) and nuclei’s (n) kinetic and potential energies, in order: the electrons kinetic energy; the nuclei kinetic energy; the electron–electron interaction potential energy; the electron–nuclei interaction potential energy; the nuclei–nuclei interaction potential energy. This Hamiltonian is really complex and it can be simplified considering that the proton mass is >103 times larger than the electron mass. As a consequence, it can be assumed that the electrons’ motion is much faster than the nuclei’s motion and that each electron explores a slowly varying configuration of the nuclei. Such “adiabatic” approximation is usually known as Born–Oppenheimer approximation [5, 8, 15, 17]. It assumes that the nuclei are practically fixed in space during the electrons’ motion, influencing the latter's energy statically. On the other side, the nuclei experience the electrons’ motion as an average value since the latter instantaneously adapt themselves to the given nuclear configuration. Such rapid rearrangement imposes that the nuclear energy is essentially related to the instantaneous nuclei positions. This enables to define a nuclear configuration and associate to it the overall electrons–nuclei system energy. Under this approximation, a configurational energy can be introduced

      (1.82)equation

      where the configurational potential energy and the kinetic energy of the nuclei are explicitly reported. In the harmonic approximation, U conf is simplified as a quadratic function of the generalized coordinate Q [15, 18]. This is the internuclear distance in the most simple diatomic molecule or a normal coordinate in the case of a polyatomic molecule [5, 7]. It can be written

      where the equilibrium position (minimum of the potential energy) Q = 0 has been chosen for simplicity and m and ω are the mass and frequency of the oscillation mode whereas U g is a constant representing the minimum energy of the given electronic configuration (related to spin and orbital motion of electrons). The complete Hamiltonian then becomes

      (1.84)equation

Image described by caption

      Each parabola schematizes the energy of the electronic configuration. In the lower parabola, representing the ground state of the system, the electrons have given spin and orbital angular momenta. In the upper parabola, schematizing the first excited state, the spin and orbital angular momenta have in general changed. The parabolic approximation gives the shape of the total energy, and the solutions of the harmonic oscillator define the possible quantized energy for the nuclear motion (represented by dashed lines in the figure). This means that not all the energy values are possible but just those marked by the dashed lines. Anyway, the energy of vibration is much lower than the energy of electrons’ interaction, and almost a continuous change can be considered within the given parabola, schematizing the electron configuration.

      Considering the excited energy level, it is characterized, in general, by a configuration coordinate of equilibrium Q = Qe different with respect to the electronic ground state. Assuming again a harmonic approximation, the total energy of the excited state can be written as