Gary A. Mabbott

Electroanalytical Chemistry


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One might say that the electric potential of electrons in the ground is zero, but that is really just a statement about their relative energy; it does not represent an absolute value. (Furthermore, the ground is really just a local benchmark, because small variations in the electrical potential can be found at different places around the earth. Fortunately, a local reference is adequate for most practical situations.).

      In electrochemical experiments, the reference potential is established by the use of a reference electrode. It is common practice to refer to a potential or voltage at an electrode when in actuality the value being discussed is the electric potential difference between the electrode in question and the reference electrode being used in that experiment. In older literature, this potential is also called the electromotive force or EMF as it is the energy available to drive charges from one point to the other and do work. Properties of reference electrodes are discussed in chapter 2 (section 2.3.4.3).

      1.2.1 Volt Defined

      (1.1)

      The volt is the unit of electric potential energy per unit charge that one normally uses with simple meters in the laboratory. So, whenever someone refers to a voltage at some part of their system, they are describing the electric potential difference between that point and some reference point (usually the ground). The voltage is the number of joules released or spent in moving a coulomb of charge from the reference point to the point in question.

      It is important to remember that the potential is the electrical work done per unit charge. However, a coulomb is a rather large amount of charge compared to the charge on a single electron. If moving a coulomb of charge from point A to point B costs 1.00 J of energy, then how much energy is required to move a single positively charged particle between the same points? First, one can calculate charge in coulombs/electron using Faraday's constant, F, the number of coulombs per mole of electrons, 9.6485 x 104 C/mol, together with Avogadro's number.

      (1.2)

      This value is the charge on an electron and is known as the elementary charge. One can calculate the energy that would be required to move a single electron through a voltage difference of 1 V by multiplying the elementary charge by 1 V in the units of 1 J/C:

      (1.3)

      The result of this calculation is frequently useful and provides the definition for a separate unit of electric potential energy per elementary charge, namely, the electron‐volt, eV.

      (1.4)

      1.2.2 Current Defined

      Current describes the movement of charge. It is the measure of the rate of change in charge moving past a specific observation point.

      (1.5)

      (1.6)

      If one were to make the analogy of an electrical circuit with a river, then the current in amperes or coulombs per second parallels the volume flow rate of the river in gallons per second. The potential energy difference or voltage that is associated with any given component (such as an electrode in an electrochemical experiment) in the electrical circuit, is analogous to the energy available to do work per gallon of water as it drops over a waterfall. Current describes the rate of charge moving (amount per unit of time) and potential is a measure of the energy per unit charge in moving between two points.

      1.2.3 Oxidation and Reduction

      The exchange of electrons between two chemical species is generally known as an oxidation/reduction process or redox reaction. In a redox reaction occurring in a homogeneous solution, one reactant gains electrons while the other reactant loses. It is often useful to consider a redox reaction from the perspective of one of the reactants. Consider a redox reaction between cerium and iron ions in aqueous solution:

      (1.7)

      The net reaction equation does not show any electrons as either reactants or products. However, it is useful to separate the two reactants into “half reactions” where electrons do appear.

      (1.8)

      (1.9)

      A process in which a chemical species accepts one or more electrons is known as a reduction reaction; a process in which a species loses electrons is an oxidation reaction. Writing the half reactions indicates that the Fe2+ ion is being oxidized and the Ce4+ ion is being reduced. It also clearly states how many electrons are being transferred per mole of a given reactant.

      1.2.4 Current and Faraday's Law